Author Topic: Degassing of Dielectric Oil Using High Vacuum.  (Read 2813 times)

Patrick

  • Guest
Degassing of Dielectric Oil Using High Vacuum.
« on: November 07, 2019, 04:32:39 AM »
Ok I'm getting ready to make a serious go at it. Some questions I have would be temp, duration, and pressure Im continuing research but not sure.

The goals for this apparatus are to degas oils and epoxy, vacuum draw and fill caps and transformers with epoxy, oil or 2 part silicone. Side projects would be to verify capacitors and mosfets at the equivalent to 100k feet at high and low temperatures.

pics of the apparatus:
https://i.imgur.com/1iv0TPR.jpg
and:
https://i.imgur.com/g2EIR0N.jpg
pdf: Attached

I'm making a stainless steel screen like layer-cake to act as Raschig rings. Which will be lifted into and out of the oil being degassed by stepper motor and scavenged 3D printer vertical axis parts. All parts will be thoroughly sonic cleaned including the motor. Ive found this and similar information that suggest .1 to 5 torr or thereabouts is a good starting point.

ill verify a samples breakdown potential before and after treatment in 6 hour intervals i guess to graph a trend indicating the end of improvement for each oil type.

I don't have access to the purpose made dielectric oil like Shell Dialla AX, but I use food oil mostly anyway.

The capacitors in the clear cube were at 100k feet for balloon testing.

.
« Last Edit: November 07, 2019, 05:30:41 AM by Patrick »

Offline davekni

  • Executive Board Member
  • *******
  • Posts: 2745
  • Karma: +130/-1
  • Physicist, engineer (electronic), and hobbiest
    • View Profile
Re: Degassing of Dielectric Oil Using High Vacuum.
« Reply #1 on: November 08, 2019, 03:52:11 AM »
Do you have oil for your vacuum pump?  That would likely be much better than food oil.  Mineral oil is often available at local stores - used as an occasional laxative or as baby oil.  (Baby oil is just mineral oil with perfume added.)  Food oils have polar groups, which will cause higher dielectric loss, more water absorption, and likely lower breakdown voltage.  Also, food oils (unless 100% saturated) have C=C double bonds, so will chemically degrade faster.
David Knierim

Patrick

  • Guest
Re: Degassing of Dielectric Oil Using High Vacuum.
« Reply #2 on: November 08, 2019, 07:02:46 PM »
mmmm Ive looked at this before, back on 4hv. ill have to run a table and chart of all oils and properties, now I have the equipment to do so. Only Corn oil seemed to be catastrophically unusable right from the get go. We were trying to stay away from hydrocarbon oils.

Soy bean oil is used in 50kV+ main line transformers which run for decades. So we always discussed this, but now we'll know. Aging is always a concern, but for me 2-3 years is fine.

We always thought "Envirotemp"was soy bean oil with green dye and 1 or 2 % additives that we hobbyists probly dont need.
https://www.cargill.com/news/releases/2013/NA3082422.jsp
« Last Edit: November 08, 2019, 07:07:15 PM by Patrick »

Offline DashApple

  • High Voltage Enthusiast
  • *
  • Posts: 29
  • Karma: +1/-0
    • View Profile
Re: Degassing of Dielectric Oil Using High Vacuum.
« Reply #3 on: November 08, 2019, 10:16:14 PM »
I have ever only vacuumed a transformer under oil to remove the trapped air within the windings and not tried to degas the oil its self so not sure if this reply will be helpful

I used HV transformer mineral oil and ran it direct from the vacuum pump for 6 days

I believe there are some baby oils that are pure mineral oil without any additives ?

Offline davekni

  • Executive Board Member
  • *******
  • Posts: 2745
  • Karma: +130/-1
  • Physicist, engineer (electronic), and hobbiest
    • View Profile
Re: Degassing of Dielectric Oil Using High Vacuum.
« Reply #4 on: November 09, 2019, 03:20:09 AM »
Interesting information about Cargill's FR3 oil derived from soybean oil.  Looks like I'm way out-of-date!  I wonder how much modification is done to the soybean oil.  They mention paper insulation lasting much longer.  Perhaps that's tied to the polar molecules in paper bonding to the polar parts of the oil.  (The dielectric dissipation caused by the polar parts of the oil would be of no issue at line frequency, only for high-frequency use.)

Cargill mentions FR3's biodegradability.  To me, that suggests the double-bonds (unsaturation) are likely still present.  Guess that's not an issue as long as the air is thoroughly removed.

Thank you for the update.  I stand corrected.
David Knierim

Patrick

  • Guest
Re: Degassing of Dielectric Oil Using High Vacuum.
« Reply #5 on: November 09, 2019, 06:54:09 AM »
I stand corrected.

Im not saying thats fact just that was an example i found from the $$$ industry.

we need this info too but i cant find any open-source or open-method examples in several years of searching. Just random YouTube vids showing a poorly wound and insulated flyback in a food container of oil.

High Voltage Forum

Re: Degassing of Dielectric Oil Using High Vacuum.
« Reply #5 on: November 09, 2019, 06:54:09 AM »

 


* Recent Topics and Posts

post Re: Capacitor in Parallel with Primary Coil
[Beginners]
Mads Barnkob
Today at 10:17:34 AM
post Capacitor in Parallel with Primary Coil
[Beginners]
FPS
Today at 10:01:41 AM
post Re: Re-chargeable 1.5 volt lithium ion AAA batteries
[General Chat]
MRMILSTAR
Today at 04:47:35 AM
post Re: Re-chargeable 1.5 volt lithium ion AAA batteries
[General Chat]
davekni
Today at 03:59:27 AM
post Re: Kaizer VTTC 1
[Vacuum Tube Tesla Coils (VTTC)]
MRMILSTAR
March 28, 2024, 09:15:11 PM
post Re: capacitor and diodes. Voltage values for a CW
[Voltage Multipliers]
Alberto
March 28, 2024, 01:01:12 PM
post Re: Big Coil Build Log
[Dual Resonant Solid State Tesla coils (DRSSTC)]
flyingperson23
March 28, 2024, 05:47:34 AM
post Re: capacitor and diodes. Voltage values for a CW
[Voltage Multipliers]
davekni
March 28, 2024, 04:45:07 AM
post Re: capacitor and diodes. Voltage values for a CW
[Voltage Multipliers]
MRMILSTAR
March 28, 2024, 04:18:27 AM
post Push Pull VTTC
[Vacuum Tube Tesla Coils (VTTC)]
janno288
March 28, 2024, 01:10:08 AM
post Re: capacitor and diodes. Voltage values for a CW
[Voltage Multipliers]
Alberto
March 27, 2024, 10:54:52 PM
post Re: CM400 Induction Heater
[Electronic Circuits]
markus
March 27, 2024, 11:53:42 AM
post Re: OCD Triggering Early + Low Output
[Dual Resonant Solid State Tesla coils (DRSSTC)]
davekni
March 27, 2024, 05:14:36 AM
post Re: Is the UD2.7C under voltage lock out basically worthless?
[Dual Resonant Solid State Tesla coils (DRSSTC)]
davekni
March 27, 2024, 04:47:48 AM
post Re: DRSSTC Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
davekni
March 27, 2024, 04:41:59 AM
post Re: DRSSTC Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
alan sailer
March 27, 2024, 12:04:34 AM
post Re: Super flat QCW simulation (does this look reasonable?)
[Dual Resonant Solid State Tesla coils (DRSSTC)]
toooldforthis
March 26, 2024, 11:08:14 PM
post Re: DRSSTC Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Benjamin Lockhart
March 26, 2024, 11:07:20 PM
post Re: Is the UD2.7C under voltage lock out basically worthless?
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Benjamin Lockhart
March 26, 2024, 10:46:29 PM
post OCD Triggering Early + Low Output
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Saattvik24
March 26, 2024, 09:03:43 PM
post Re: DRSSTC Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
alan sailer
March 26, 2024, 08:46:59 PM
post Re: DRSSTC Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
flyingperson23
March 26, 2024, 05:02:18 PM
post Re: DRSSTC Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
alan sailer
March 26, 2024, 03:16:03 PM
post Re: CM400 Induction Heater
[Electronic Circuits]
Anders Mikkelsen
March 26, 2024, 01:41:49 PM
post Re: Benjamin's DRSSTC 2 in progress
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Benjamin Lockhart
March 26, 2024, 04:48:22 AM
post Re: Re-chargeable 1.5 volt lithium ion AAA batteries
[General Chat]
MRMILSTAR
March 26, 2024, 04:16:37 AM
post Re: DRSSTC Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
davekni
March 26, 2024, 04:16:24 AM
post Re: Smoke Screen Machine Protect 950 XP - Teardown of a Smoke Cannon!
[Electronic Circuits]
davekni
March 26, 2024, 04:13:02 AM
post Re: CM400 Induction Heater
[Electronic Circuits]
davekni
March 26, 2024, 04:00:43 AM
post Re: Re-chargeable 1.5 volt lithium ion AAA batteries
[General Chat]
davekni
March 26, 2024, 03:19:18 AM
post Re: Benjamin's DRSSTC 2 in progress
[Dual Resonant Solid State Tesla coils (DRSSTC)]
thedoc298
March 26, 2024, 01:50:42 AM
post Re: DRSSTC Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
flyingperson23
March 25, 2024, 08:05:02 PM
post Re: Smoke Screen Machine Protect 950 XP - Teardown of a Smoke Cannon!
[Electronic Circuits]
Mads Barnkob
March 25, 2024, 07:41:29 PM
post Re: DRSSTC Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
alan sailer
March 25, 2024, 06:45:46 PM
post Re: DRSSTC Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
flyingperson23
March 25, 2024, 05:44:25 PM
post Re: CM400 Induction Heater
[Electronic Circuits]
Anders Mikkelsen
March 25, 2024, 04:47:17 PM
post Re: DRSSTC Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
alan sailer
March 25, 2024, 04:27:22 PM
post Re-chargeable 1.5 volt lithium ion AAA batteries
[General Chat]
MRMILSTAR
March 25, 2024, 03:57:34 PM
post Re: CM400 Induction Heater
[Electronic Circuits]
markus
March 25, 2024, 02:06:41 PM
post Re: Odd MOSFET Driver Behavior
[Solid State Tesla Coils (SSTC)]
KrisPringle
March 25, 2024, 04:43:25 AM
post Re: Odd MOSFET Driver Behavior
[Solid State Tesla Coils (SSTC)]
davekni
March 25, 2024, 02:39:40 AM
post Re: Odd MOSFET Driver Behavior
[Solid State Tesla Coils (SSTC)]
KrisPringle
March 25, 2024, 12:47:09 AM
post Re: capacitor and diodes. Voltage values for a CW
[Voltage Multipliers]
Alberto
March 24, 2024, 07:36:32 PM
post Re: My completed 14-stage Cockroft-Walton voltage multiplier
[Voltage Multipliers]
Alberto
March 24, 2024, 07:27:24 PM
post Re: capacitor and diodes. Voltage values for a CW
[Voltage Multipliers]
MRMILSTAR
March 24, 2024, 04:25:23 AM
post Re: capacitor and diodes. Voltage values for a CW
[Voltage Multipliers]
Alberto
March 23, 2024, 10:47:35 PM
post Re: capacitor and diodes. Voltage values for a CW
[Voltage Multipliers]
MRMILSTAR
March 23, 2024, 09:30:21 PM
post Re: capacitor and diodes. Voltage values for a CW
[Voltage Multipliers]
Alberto
March 23, 2024, 04:34:31 PM
post Re: capacitor and diodes. Voltage values for a CW
[Voltage Multipliers]
MRMILSTAR
March 23, 2024, 03:04:25 PM
post Re: capacitor and diodes. Voltage values for a CW
[Voltage Multipliers]
Alberto
March 23, 2024, 01:38:34 PM
post Re: capacitor and diodes. Voltage values for a CW
[Voltage Multipliers]
MRMILSTAR
March 23, 2024, 04:20:03 AM
post Re: Welcome new members, come say hello and tell a little about yourself :)
[General Chat]
davekni
March 23, 2024, 12:54:30 AM
post Re: Smoke Screen Machine Protect 950 XP - Teardown of a Smoke Cannon!
[Electronic Circuits]
davekni
March 23, 2024, 12:05:57 AM
post capacitor and diodes. Voltage values for a CW
[Voltage Multipliers]
Alberto
March 22, 2024, 11:45:03 PM
post Re: Welcome new members, come say hello and tell a little about yourself :)
[General Chat]
OmGigaTron
March 22, 2024, 11:30:09 PM
post Smoke Screen Machine Protect 950 XP - Teardown of a Smoke Cannon!
[Electronic Circuits]
Mads Barnkob
March 22, 2024, 10:20:35 PM
post Re: Where's all this voltage coming from?
[Spark Gap Tesla Coils (SGTC)]
Benbmw
March 22, 2024, 09:21:13 PM
post Re: What actually kills MOSFETs?
[Beginners]
AstRii
March 22, 2024, 03:37:11 PM
post What actually kills MOSFETs?
[Beginners]
FPS
March 22, 2024, 05:09:20 AM
post Re: Benjamin's DRSSTC 2 in progress
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Benjamin Lockhart
March 22, 2024, 03:57:54 AM
post Re: Benjamin's DRSSTC 2 in progress
[Dual Resonant Solid State Tesla coils (DRSSTC)]
davekni
March 22, 2024, 02:59:25 AM
post Re: Benjamin's DRSSTC 2 in progress
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Benjamin Lockhart
March 21, 2024, 06:31:42 PM
post Re: 2x Panasonic Inverter Microwaves - what to salvage, dangers?
[General Chat]
rikkitikkitavi
March 21, 2024, 03:08:01 PM
post Re: [WTS] IGBT, Ferrite, Capacitors, Tools, PSU, Industrial components and parts
[Sell / Buy / Trade]
Mads Barnkob
March 21, 2024, 01:37:32 PM
post Re: Difference between these transformers
[Transformer (Ferrite Core)]
Alberto
March 21, 2024, 11:42:07 AM
post Re: Phase Lead Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
davekni
March 21, 2024, 04:09:14 AM
post Re: Benjamin's DRSSTC 2 in progress
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Benjamin Lockhart
March 21, 2024, 02:15:31 AM
post My Homemade Structural Analysis X-Ray Machine
[X-ray]
Luca c.
March 21, 2024, 01:35:40 AM
post Re: Phase Lead Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Saattvik24
March 20, 2024, 10:40:00 PM
post Re: Difference between these transformers
[Transformer (Ferrite Core)]
Mads Barnkob
March 20, 2024, 08:03:41 PM
post Re: 2x Panasonic Inverter Microwaves - what to salvage, dangers?
[General Chat]
Mads Barnkob
March 20, 2024, 07:51:57 PM
post Re: Benjamin's DRSSTC 2 in progress
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Mads Barnkob
March 20, 2024, 10:39:47 AM
post Re: Phase Lead Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
davekni
March 20, 2024, 04:09:59 AM
post Re: 160mm DRSSTC II project | Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Benjamin Lockhart
March 20, 2024, 01:13:23 AM
post Re: Phase Lead Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Keybored
March 20, 2024, 12:45:16 AM
post Re: Benjamin's DRSSTC 2 in progress
[Dual Resonant Solid State Tesla coils (DRSSTC)]
flyingperson23
March 20, 2024, 12:30:30 AM
post Re: Benjamin's DRSSTC 2 in progress
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Benjamin Lockhart
March 19, 2024, 11:12:24 PM
post Re: 160mm DRSSTC II project | Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Late
March 19, 2024, 09:47:49 PM
post Re: 160mm DRSSTC II project | Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Late
March 19, 2024, 09:44:19 PM
post Phase Lead Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Saattvik24
March 19, 2024, 06:52:09 PM
post Re: 160mm DRSSTC II project | Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
flyingperson23
March 19, 2024, 05:02:44 PM
post Re: Welcome new members, come say hello and tell a little about yourself :)
[General Chat]
Mads Barnkob
March 19, 2024, 05:01:41 PM
post Re: Benjamin's DRSSTC 2 in progress
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Mads Barnkob
March 19, 2024, 04:31:02 PM
post Re: 160mm DRSSTC II project | Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Mads Barnkob
March 19, 2024, 03:59:54 PM
post Re: Benjamin's DRSSTC 2 in progress
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Benjamin Lockhart
March 19, 2024, 06:41:39 AM
post Re: Welcome new members, come say hello and tell a little about yourself :)
[General Chat]
davekni
March 19, 2024, 04:05:49 AM
post Re: Welcome new members, come say hello and tell a little about yourself :)
[General Chat]
OmGigaTron
March 18, 2024, 09:08:35 PM
post Re: Can I Trust This Super Cheap Site?
[General Chat]
2020-Man
March 18, 2024, 09:07:35 PM
post Re: Can I Trust This Super Cheap Site?
[General Chat]
Twospoons
March 18, 2024, 08:57:06 PM
post Re: Can I Trust This Super Cheap Site?
[General Chat]
MRMILSTAR
March 18, 2024, 03:51:33 PM
post Re: 160mm DRSSTC II project | Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Late
March 18, 2024, 02:59:46 PM
post Re: 160mm DRSSTC II project | Questions
[Dual Resonant Solid State Tesla coils (DRSSTC)]
Late
March 18, 2024, 02:33:25 PM
post Can I Trust This Super Cheap Site?
[General Chat]
2020-Man
March 18, 2024, 11:02:12 AM
post Re: Where's all this voltage coming from?
[Spark Gap Tesla Coils (SGTC)]
Twospoons
March 18, 2024, 02:36:11 AM
post Re: Best forum for vacuum tube amplifiers?
[General Chat]
Mads Barnkob
March 17, 2024, 07:42:55 PM
post Re: 2x Panasonic Inverter Microwaves - what to salvage, dangers?
[General Chat]
Michelle_
March 17, 2024, 04:15:14 PM
post Re: 2x Panasonic Inverter Microwaves - what to salvage, dangers?
[General Chat]
Michelle_
March 17, 2024, 05:05:04 AM
post Re: Where's all this voltage coming from?
[Spark Gap Tesla Coils (SGTC)]
davekni
March 17, 2024, 04:50:51 AM
post Re: 2x Panasonic Inverter Microwaves - what to salvage, dangers?
[General Chat]
Twospoons
March 17, 2024, 04:45:17 AM
post 2x Panasonic Inverter Microwaves - what to salvage, dangers?
[General Chat]
Michelle_
March 17, 2024, 04:17:51 AM

Sitemap 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 
SimplePortal 2.3.6 © 2008-2014, SimplePortal